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On May 21, 1998, PharmaPrint, Inc. reported traces of the fungicide quintozene (pentachloronitrobenzene, PCNB ) in raw ginseng root to the FDA.  PharmaPrint is developing herbal products.  Supplement makers using herbal products are advised to monitor for PCNB and the related pesticide hexachlorobenzene (HCB).

pentachlorobenzene

hexachlororbenzene

pentachloronitrobenzene (PCNB)

hexachlorobenzene (HCB)

Analysis of PCNB and HCB

We offer PCNB and HCB analysis along with other pesticides.  The analysis is conducted using dual capillary column gas chromatography with electron capture detection (GC ECD).   The presence of a pesticide is automatically confirmed by retention times on two separate, dissimilar GC columns.  Detection limits in herbal products is usually 1-10 ug/kg.   For a quotation ...

PCNB and HCB analysis

The levels of PCNB and HCB have been found to be as high as 1-20 mg/kg in some herbs.   For information on the health risks of PCNB, contact FDA or Robert McCaleb of the Herb Research Foundation at 303-449-2265.

We also offer pesticide analysis by GCMS to either confirm the GC analysis or to separately quantitate the pesticide using selected ion monitoring (SIM).

 

PCNB analysis by GCMS

Exova

9240 Santa Fe Springs Rd
Santa Fe Springs, CA 90670

info400@exova.com

562.948.2225 Fax 562.948.5850

Exova

Formerly West Coast Analytical Service (WCAS) and Bodycote Testing Group